HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotriethylsilane → n,n-Diethyl-2-chloro-6-(triethylsilyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotriethylsilane | HCID 13819 | — |
| Reactant | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| Product | n,n-Diethyl-2-chloro-6-(triethylsilyl)benzamide | HCID 18630182 | — |
Reaction Steps
The title compound was prepared according to General Method A from the compound of Example e and 1.4 eq chlorotriethylsilane. Purification by HPLC with 1:19 ethyl acetate/hexanes gave 6.0 g of the desired product as a clear oil, a 92% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248894B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-7c7bba4a800747729ff5b7330a265047 |
| Source note | uspto-grants-2001_06 |