Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 70239688 | HCID 70239688 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70204049 | HCID 70204049 | — |
Reaction Steps
To a solution of trans-N-t-butoxycarbonyl-4-(3-methylphenyl)-3 methoxy piperidine, (0.20 g, 0.65 mmol) in EtOAc (50 ml) at 0° C. was bubbled HCl gas until saturated. The reaction was stirred at 0° C. for 10 min and then the solvent evaporated in vacuo to afford the product as a white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06248756B1 |
|---|
| Source dataset | uspto-grants-2001_06 |
|---|
| ORD ID | ord-89350ddf94b94dc98560f3d1c6de7635 |
|---|
| Source note | uspto-grants-2001_06 |
|---|
