HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21193217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21193209 | HCID 21193209 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21193217 | HCID 21193217 | — |
Reaction Steps
A solution of N-tert-butoxycarbonyl-4-methoxymethyl-4-(3-tolylsulfanyl)piperidine (0.18 g) in ethyl acetate (25 mL) at 0° C. was saturated with hydrogen chloride gas. The resultant solution was stirred at 0° C. for one h. The product solution was concentrated under vacuum to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248756B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-ea3b50d5500148e8beec76e6a76478cf |
| Source note | uspto-grants-2001_06 |