HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → Benzene, [(trichlorosilyl)methyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Tributylamine | HCID 7622 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Product | Benzene, [(trichlorosilyl)methyl]- | HCID 69863 | 29% |
Reaction Steps
In the same apparatus and procedure as Example 1 above, 0.090 g (0.5 mmol) of tri-n-butylamine, 0.63 g (5.0 mmol) of benzyl chloride, and 3.41 g (25.2 mmol) of trichlorosilane were reacted at 150° C. for 6 hrs. The resulting mixture was distilled to give 0.32 g of benzyltrichlorosilane (yield; 29%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251057B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-fdbd087bf1b8404682147f6309557694 |
| Source note | uspto-grants-2001_06 |