HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21190249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21190149 | HCID 21190149 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21190249 | HCID 21190249 | 100% |
Reaction Steps
In a mixture of 10 ml of ethanol and 1 ml of 12N HCl was dissolved 542 mg (1.34 mmol) of 4,5-dihydro-2-ethyl-4-(5-trifluoromethanesulfonamidopentan-1-yl)-3H-1,4,8b-triazaacenaphthylene. The solvent was distilled off under reduced pressure to leave 640 mg of the desired compound (100%, white amorphous substance).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251905B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-4c9b814359b646b5aa7772e64918de6e |
| Source note | uspto-grants-2001_06 |