Water → HCID 10924661, compound

Participants

Reaction Steps

29.7 g (0.13 mol) of 2-vinylnaphthalene, 25 g (0.16 mol) of ethyl 2-bromobenzoate, 22.5 ml (0.16 mol) of triethylamine, 0.54 g of palladium diacetate and 1.44 g of triphenylphosphine in 200 ml of acetonitrile were heated to 100° C. for 20 h. The reaction mixture was then poured into water and the mixture was extracted repeatedly with ethyl acetate. The organic phase was concentrated under reduced pressure and the residue was purified chromatographically on silica gel. 34 g (71%) of the product were obtained.

Provenance & Evidence