HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylbenzoic Acid → HCID 10194429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylbenzoic Acid | HCID 11470 | — |
| Reactant | 2,4-Dimethoxy-5-(2-methyl-thiazol-4-yl)-benzaldehyde | HCID 21981121 | — |
| Product | HCID 10194429 | HCID 10194429 | — |
Reaction Steps
The title compound was prepared by condensing 2,4-dimethoxy-5-(2-methyl-thiazol-4-yl)-benzaldehyde (Ex-69A) and 4-acetylbenzoic acid in a similar manner as described in Ex-3. Yellow solid, mp 201–202° C. (dec.). 1H-NMR (DMSO-d6) δ 8.47 (s, 1H), 8.14–7.97 (m, 5H), 7.76 (s, 1H), 7.65 (d, J=15.8 Hz, 1H), 6.81 (s, 1H), 4.00 (s, 3H), 3.98 (s, 3H), 2.69 (s, 3H). MS m/z=409 (M+, 70%), 378 ([M−OCH3]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094801B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-de02eab211fe46eb88ec524083dacd35 |
| Source note | uspto-grants-2006_08 |