HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenylboronic Acid → HCID 53657704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenylboronic Acid | HCID 1677 | — |
| Reactant | Ethyl 5-bromopyridine-3-carboxylate | HCID 140785 | — |
| Catalyst | HCID 178420553 | HCID 178420553 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53657704 | HCID 53657704 | — |
Reaction Steps
n.m.r. δ values include 1.5 (t, 3 H), 4.5 (q, 2 H), 7.75 (t, 1 H), 8.0 (d, 1 H), 8.3 (d, 1 H), 8.6-8.5 (m, 2 H), 9.0 (s, 1 H), 9.3 (s, 1 H); from 3-bromo-5-pyridine carboxylic acid ethyl ester (985 mg) in toluene (15 mL), tetrakis(triphenylphosphino)palladium(0) (161 mg) and 3-nitrophenylboronic acid (860 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251925B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-8fbcb33a8b964ac2903d328b687e9c23 |
| Source note | uspto-grants-2001_06 |