HCID 11615843, compound → HCID 11572141, compound

HRID 1069080Notes

Reaction equation

HRID 1069080 reaction equation
[CH3:1][O:2][C:3]([C:5]1[C:6]([C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-])=O)[CH:12]=2)=[N:7][CH:8]=[CH:9][CH:10]=1)=[O:4]>[Pd]>[CH3:1][O:2][C:3]([C:5]1[C:6]([C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([NH2:17])[CH:12]=2)=[N:7][CH:8]=[CH:9][CH:10]=1)=[O:4]

Participants

3

Reactant 1

HCID 11615843HCID 11615843, compound

Product 1

HCID 11572141HCID 11572141, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

n.m.r. (DMSO-d6) δ values include 3.65 (s, 3 H), 5.19 (s, 2 H), 6.58 (dt, 2 H), 6.76 (s, 1 H), 7.05 (t, 1 H), 7.44 (dd, 1 H), 8.02 (d, 1 H), 8.73 (d, 1 H); from 2-(3-nitrophenyl)-3-pyridinecarboxylic acid methyl ester (293 mg) and 10% Pd/C (30 mg).

Sources & evidence

ORD record
ord-6e319a43f71b4f299468ba6dfa0c05ca
Source dataset
uspto-grants-2001_06
Patent number
US06251925B1

Reaction notes

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