HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69780311, compound → HCID 69780319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69780311 | HCID 69780311 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69780319 | HCID 69780319 | — |
Reaction Steps
Assay Found: C 55.95; H 5.26; N 4.98%; C26H27Cl1N2O5.2HCl requires C 56.18; H 5.26; N 5.04%; from (R)-3′-[[2-[[2-(3-chlorophenyl)-2-[[(tert-butyl)dimethylsilyl]oxy]ethyl][(tert-butoxy)carbonyl]amino]ethyl]amino]-[1,1′-biphenyl]-2,4-dicarboxylic acid dimethyl ester (508 mg) in 4 N hydrochloric acid in dioxane (10 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251925B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-3e08c92fe5ee47a987e1c6e620b92c9d |
| Source note | uspto-grants-2001_06 |