Rhodanine → HCID 86752514, compound

HRID 1069136Notes

Reaction equation

HRID 1069136 reaction equation
[CH2:1]([C:6]1[CH:20]=[CH:19][C:9]([O:10][C:11]2[CH:12]=[C:13]([CH:16]=[CH:17][CH:18]=2)[CH:14]=O)=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[S:21]1[CH2:27][C:25](=[O:26])[NH:24][C:22]1=[S:23]>C(O)(=O)C.C([O-])(=O)C.[Na+]>[CH2:1]([C:6]1[CH:20]=[CH:19][C:9]([O:10][C:11]2[CH:12]=[C:13]([CH:14]=[C:27]3[S:21][C:22](=[S:23])[NH:24][C:25]3=[O:26])[CH:16]=[CH:17][CH:18]=2)=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

5

Reactant 2

HCID 1201546RhodanineHCID 21191289HCID 21191289, compound

Product 1

HCID 86752514HCID 86752514, compoundYield 61.9%

Reagents, catalysts & solvents 2

HCID 176Acetic AcidSolventHCID 517045Sodium AcetateSolvent

Procedure

The 3-(4-n-pentylphenoxy)benzaldehyde was coupled with rhodanine in acetic acid and sodium acetate essentially as described previously to yield 1.3 grams (61.9%) of the title product.

Sources & evidence

ORD record
ord-84550ca5db2c4c7081585263b6cc5461
Source dataset
uspto-grants-2001_06
Patent number
US06251928B1

Reaction notes

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