4-Fluorobenzyl bromide → HCID 86757062, compound

HRID 1069431Notes

Reaction equation

HRID 1069431 reaction equation
[CH3:1][C:2]1[N:7]([CH2:8][C:9]([O:11][CH3:12])=[O:10])[C:6](=[O:13])[C:5]([N+:14]([O-:16])=[O:15])=[C:4](OS(C(F)(F)F)(=O)=O)[CH:3]=1.[F:25][C:26]1[CH:31]=[CH:30][C:29]([CH2:32]Br)=[CH:28][CH:27]=1>>[F:25][C:26]1[CH:31]=[CH:30][C:29]([CH2:32][C:4]2[CH:3]=[C:2]([CH3:1])[N:7]([CH2:8][C:9]([O:11][CH3:12])=[O:10])[C:6](=[O:13])[C:5]=2[N+:14]([O-:16])=[O:15])=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 680214-Fluorobenzyl bromideHCID 11079278Methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate

Product 1

HCID 86757062HCID 86757062, compound

Procedure

This compound is prepared from 11 g (29.4 mmol) of methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate and 10 g (52.9 mmol) of (4-fluorophenyl)-methyl bromide according to the method described in 1.5.

Sources & evidence

ORD record
ord-abce9b5f1a87417ab6ce9a7277f12b6a
Source dataset
uspto-grants-2001_06
Patent number
US06252082B1

Reaction notes

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