HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloroformate → HCID 70186121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | HCID 70186099 | HCID 70186099 | — |
| Product | HCID 70186121 | HCID 70186121 | 57% |
Reaction Steps
1.12 g (3.83 mmol of methyl 3-amino-4-(cyclohexylmethyl)-6-methyl-2-oxo-1,2-dihydropyridine-1-acetate are reacted with phenylmethyl chloroformate under the conditions described in Example 3. 0.93 g of product is obtained after purification by chromatography on a silica gel column, eluting with a dichloromethane:methanol (98:2) mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252082B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-af1dbbe7f9d14a369a850490d5eeb6b7 |
| Source note | uspto-grants-2001_06 |