HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → Methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 10688397 | HCID 10688397 | — |
| Reactant | HCID 10829831 | HCID 10829831 | — |
| Product | Methanol | HCID 887 | 67% |
| Product | HCID 10829831 | HCID 10829831 | — |
Reaction Steps
5-Methoxy-2-methyl-1-[(2-pyridyl)methyl]-1H-indole-3-acetic acid hydrazide. Using the method described in Example 6, Part B, 480 mg 1.4 mmol) of 5-methoxy-2-methyl-1-[(2-pyridyl)methyl]-1H-indole-3-acetic acid ethyl ester was reacted with 1.4 mL of hydrazine to give on crystallization from MeOH 304 mg (67% yield) of 5-methoxy-2-methyl-1-[(2-pyridyl)methyl]-1H-indole-3-acetic acid hydrazide, mp, 147-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252084B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-00b39acddbe440a7bb4e9b7da5c9e867 |
| Source note | uspto-grants-2001_06 |