HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 10568956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Methyl 2-ethyl-5-methoxy-1-(phenylmethyl)-1H-indole-3-acetate | HCID 10497168 | — |
| Product | HCID 10568956 | HCID 10568956 | 74% |
Reaction Steps
Using the method described in Example 3, Part C, 748 mg 2.2 mmol) of 2-ethyl-5-methoxy-1-(phenylmethyl)-1H-indole-3-acetic acid methyl ester was reacted with 2.2 mL of hydrazine to give 552 mg (74% yield) of 2-ethyl-5-methoxy-1-(phenylmethyl)-1H-indole-3-acetic acid hydrazide, that crystallized out of the reaction mixture on cooling (melting point, 138-140° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252084B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-74753ae4974d46b0b7e03255c8b4b572 |
| Source note | uspto-grants-2001_06 |