HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 10802701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 10661460 | HCID 10661460 | — |
| Product | HCID 10802701 | HCID 10802701 | — |
Reaction Steps
4-Methoxy-1-(phenylmethyl)-1H-indole-3-acetamide (236 mg, 0.8 mmol) and 3.2 mL of BBr3 were reacted as described in Example 56, Part C, go give after chromatography en silica gel (eluted with 50% ethyl acetate/hexane) 78 mg (35% yield) of 4-hydroxy-1-(phenylmethyl)-1H-indole-3-acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252084B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-b888d652d42f44f2b4963d3d9d2f612d |
| Source note | uspto-grants-2001_06 |