HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hexene → 2-Octanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hexene | HCID 11597 | — |
| Reactant | Benzyl acetone | HCID 17355 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-Octanone | HCID 8093 | — |
Reaction Steps
Under the same reaction procedure and conditions as in Example 2 (2-amino-3-pycoline 20 mol %, 150° C., 48 hours), benzyl acetone 32 mg (0.22 mmol) and 1-hexene 182 mg (2.16 were reacted in toluene 100 mg in the presence of various metal catalysts (10 mol % based on benzyl acetone). A measurement was made of the yields of 2-octanone and the results are given in Table 7, below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252118B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-9721706e34ec4359962406bc0c902671 |
| Source note | uspto-grants-2001_06 |