HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde | HCID 10829743 | — |
| Product | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol | HCID 57315820 | 93.9% |
Reaction Steps
In substantially the same manner in Reference Example 93, 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde (6.47 g) was reduced by sodium borohydride (760 mg) to obtain 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol (6.11 g, yield 93%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251926B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-0560edc9d4964f6ba42313b8b87ff9c2 |
| Source note | uspto-grants-2001_06 |