HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorobenzoic Acid → HCID 14901665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorobenzoic Acid | HCID 447 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 3-chloro-N,N-diethylbenzamide | HCID 639085 | — |
| Product | HCID 14901665 | HCID 14901665 | 95% |
Reaction Steps
N,N-diethyl-3-chlorobenzamide (10.45 g, 50 mmol) (prepared from 3-chlorobenzoic acid and diethylamine using the procedures described above) was reacted with TMSCl (16.30 g, 150 mmol) using General Method A to afford 13.4 g of the title compound as an orange oil in 95% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252078B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-4874a770cedf4f06bf3c993aa2a49784 |
| Source note | uspto-grants-2001_06 |