HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18630378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18630176 | HCID 18630176 | — |
| Product | HCID 18630378 | HCID 18630378 | — |
Reaction Steps
The title compound was prepared from the compound of Example 74 and 3.0 eq MeI according to General Method A and recrystallized from cold hexanes/ethyl acetate to give 2.5 g of the title compound, an 82% yield. m.p. 96-97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252078B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-637ca38e5bd0474380500a4109f4658d |
| Source note | uspto-grants-2001_06 |