HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 18630265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | HCID 18630276 | HCID 18630276 | — |
| Product | HCID 18630265 | HCID 18630265 | 85% |
Reaction Steps
The acid chloride prepared in Example 207 was reacted with propargylamine (3 eq) using General Method E1 to afford the title compound. Purification by recrystallization from hexanes gave 0.48 g of the title compound as an off-white solid in 85% yield. m.p. 109-111° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252078B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-43af1bc2a12a4628890acb880d89c2e9 |
| Source note | uspto-grants-2001_06 |