HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → HCID 22396185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | 175201-96-4 | HCID 9582211 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22396185 | HCID 22396185 | 96.8% |
Reaction Steps
(1Z)-N′-hydroxy-2-(2-thienylsulfonyl)ethanimidamide (0.250 g) with dihydro-2,5-furandione (0.114 g) in dimethylformamide (0.2 ml) was heated at 120° C. for 2 hours. The reaction was allowed to cool and triturated with diethyl ether and filtered to leave 3-{3-[(2-thienylsulfonyl)methyl]-1,2,4-oxadiazol-5-yl}propanoic acid (0.332 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903085B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-b049fb50241c422a90aefd5d73421358 |
| Source note | uspto-grants-2005_06 |