HRID1070530

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID713

Formamide

CH3NO

结构：Clc1ccc(Nc2nnc(OCc3ccncc3)c3ccccc23)cc1

HCID22397275

N-(4-Chlorophenyl)-4-[(pyridin-4-yl)methoxy]phthalazin-1-amine

C20H15ClN4O

PRODUCTS

生成物

结构：NC(=O)c1cc(COc2nnc(Nc3ccc(Cl)cc3)c3ccccc23)ccn1

HCID9909266

未命名化合物

收率 10%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID86759755

未命名化合物

PROCEDURE

实验过程

The general procedure used for the preparation of Example 4 was used to prepare 5 from 1-(4-chlorophenylamino)-4-(4-pyridylmethoxy)phthalazine and formamide; (10% yield). TLC (dichloromethane/acetone/triethylamine 7.5:1.0:0.5): Rf=0.42.

WORKUP

后处理

customThe general procedure used for the preparation of Example 4