Methyl 6-Bromohexanoate → 6-[3-(4-Methylphenyl)amino-4-nitrophenyl]oxyhexanoic acid methyl ester

HRID 1070850Notes

Reaction equation

HRID 1070850 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[CH:10]=[C:11]([OH:18])[CH:12]=[CH:13][C:14]=2[N+:15]([O-:17])=[O:16])=[CH:4][CH:3]=1.[CH3:19][O:20][C:21](=[O:28])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]Br>>[CH3:19][O:20][C:21](=[O:28])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][O:18][C:11]1[CH:12]=[CH:13][C:14]([N+:15]([O-:17])=[O:16])=[C:9]([NH:8][C:5]2[CH:4]=[CH:3][C:2]([CH3:1])=[CH:7][CH:6]=2)[CH:10]=1

Participants

3

Reactant 2

HCID 4170292Methyl 6-BromohexanoateHCID 222822113-(4-Methylphenyl)amino-4-nitrophenol

Product 1

HCID 673190746-[3-(4-Methylphenyl)amino-4-nitrophenyl]oxyhexanoic acid methyl ester

Procedure

990 mg of 3-(4-methylphenyl)amino-4-nitrophenol was reacted with 6-bromohexanoic acid methyl ester according to general operating instructions 2. 1.5 g was obtained.

Workup

  1. custom1.5 g was obtained

Sources & evidence

ORD record
ord-d7a1ae8f61a5451bbab678464e448833
Source dataset
uspto-grants-2005_06
Patent number
US06903126B2

Reaction notes

Loading…