HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69461265, compound → HCID 10287892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69461265 | HCID 69461265 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10287892 | HCID 10287892 | 79% |
Reaction Steps
A mixture of 150 mg (0.36 mmol) (12R,23R)-14,21-dioxa-1,8-diaza-tricyclo[21.3.0.0 8,12]hexacos-17-ene-2,7,13,22-tetraone and 20 mg 10%) palladium/carbon in 5 ml ethylacetate was hydrogenated over night. Filtration and removal of the solvent yielded 120 mg (79%) (12R,23R)-14,21-dioxa-1,8-diaza-tricyclo[21.3.0.0 8,12]hexacosane-2,7,13,22-tetraone as a light yellow oil, MS m/e (%): 423 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903129B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-e5c776758ad04a32b038afe787ba4c8f |
| Source note | uspto-grants-2005_06 |