HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69461682, compound → HCID 10127525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69461682 | HCID 69461682 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10127525 | HCID 10127525 | 61% |
Reaction Steps
A mixture of 400 mg (0.9 mmol) (12R,25R)-14,23-dioxa-1,8-diaza-tricyclo[23.3.0.0 8,12]octacos-18-ene-2,7,13,24-tetraone and 40 mg 10% palladium/carbon in 10 ml ethylacetate was hydrogenated over night. Filtration and removal of the solvent yielded 245 mg (61%) (12R,25R)-14,23-dioxa-1,8-diaza-tricyclo[23.3.0.0 8,12]octacosane-2,7,13,24-tetraone as a white solid, MS m/e (%): 451 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903129B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-669de30cf3204749946d18e3fc71209e |
| Source note | uspto-grants-2005_06 |