HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22397498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69429651 | HCID 69429651 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22397498 | HCID 22397498 | — |
Reaction Steps
The product of Step c was dissolved in dioxane (10 ml) and HCl (6N) (10 ml) was added and the reaction stirred for 3 hrs. Organic solvent was evaporated and aqueous NaOH (2M) added. The product was extracted with ethyl acetate, the combined organic extracts dried with Na2SO4 and concentrated to give the sub-title product as an oil (0.54 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903115B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-b34552ed17434d3fa6bb843d203ae19c |
| Source note | uspto-grants-2005_06 |