Diethyl Ether → HCID 178488142, compound

HRID 1071536Notes

Reaction equation

HRID 1071536 reaction equation
[CH3:1][O:2][C:3]1[CH:20]=[CH:19][C:6]2[NH:7][C:8]([S:10][CH2:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH2:18])=[N:9][C:5]=2[CH:4]=1.C([O:23]CC)C>>[CH3:1][O:2][C:3]1[CH:20]=[CH:19][C:6]2[NH:7][C:8]([S:10]([CH2:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH2:18])=[O:23])=[N:9][C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 3283Diethyl EtherHCID 178488113HCID 178488113, compound

Product 1

HCID 178488142HCID 178488142, compound

Procedure

The title compound was prepared by the method of Example 3 using 1.20 g of the title product of Example 11 instead of the title product of Example 2. Trituration with diethylether gave 1.04 g of the title compound: m.p. 147-148° C. Analysis. Calc'd. for C15H15N3O2S: C, 59.78; H, 5.02; N,13.94; S, 10.64. Found: C, 59.30; H, 4.95; N, 13.55; S, 10.73.

Sources & evidence

ORD record
ord-2891eb55710c4cf9a45d10279393f7ee
Source dataset
uspto-grants-2005_06
Patent number
US06906078B2

Reaction notes

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