Diethyl Ether → HCID 13754162, compound

Participants

Reaction Steps

The title compound was prepared by the method of Example 3 using 2.63 g of the title product of Example 25 instead of the title product of Example 2 and using 1,2-dichloroethane as solvent instead of chloroform. Trituration with diethyl ether gave 3.0 g of the title compound. Analysis. Calc'd. for C15H15N3OS: C, 63.14; H, 5.30; N, 14.73; S, 11.23. Found: C, 61.44; H, 4.98; N, 14.35; S, 11.10.

Provenance & Evidence