Diethyl Ether → HCID 69796367, compound

HRID 1071541Notes

Reaction equation

[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20].C([O:23]CC)C>>[OH2:23].[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20])=[O:23].[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20])=[O:23]

Participants

Reactant 2

HCID 3283Diethyl Ether

HCID 14064669HCID 14064669, compound

Product 1

HCID 69796367HCID 69796367, compound

Procedure

The title compound was prepared by the method of Example 3 using 950 mg of the title product of Example 29 instead of the title product of Example 2. Trituration with diethylether gave 434 mg of the title compound. Analysis. Calc'd. for C16H17N3OS*½ H2O: C, 62.23; H, 5.88; N, 13.63; S, 10.40. Found: C, 62.39; H, 5.72; N, 13.50; S, 10.65.

Sources & evidence

ORD record: ord-3973ac8daf364a899e79fc8a07499fc6
Source dataset: uspto-grants-2005_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06906078B2

Reaction notes

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