1,3-Cyclohexanedione → HCID 5224489, compound

HRID 1071785Notes

Reaction equation

HRID 1071785 reaction equation
[C:1]1(=O)[CH2:6][CH2:5][CH2:4][C:3](=[O:7])[CH2:2]1.[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([NH:16][NH2:17])=[CH:12][CH:11]=1>O>[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([NH:16][N:17]=[C:1]2[CH2:6][CH2:5][CH2:4][C:3](=[O:7])[CH2:2]2)=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 104341,3-CyclohexanedioneHCID 70624(4-Chlorophenyl)hydrazine

Product 1

HCID 5224489HCID 5224489, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 1,3-cyclohexanedione (5.05 g, 45 mmol) in water is treated over a 10 min period with an aqueous suspension of p-chlorophenylhydrazine (8.06 g, 45 mmol), stirred at room temperature for 16 h and filtered. The filtercake is washed with water and dried in vacuo to give the title product which is used as in Example 132.

Workup

  1. filtrationfiltered
  2. washThe filtercake is washed with water
  3. customdried in vacuo

Sources & evidence

ORD record
ord-ce18a14601ec4d5e9b880d4043cfb7eb
Source dataset
uspto-grants-2005_06
Patent number
US06906095B2

Reaction notes

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