HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 10120784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Trifluoroacetate | HCID 84468 | — |
| Reactant | 3-Carbamoyl-5-dipropylcarbamoyl-benzoic acid | HCID 22394891 | — |
| Reactant | HCID 59067288 | HCID 59067288 | — |
| Product | HCID 10120784 | HCID 10120784 | — |
Reaction Steps
The trifluoroacetate salt of (2S,3R,4R)-2-amino-1,7-diphenyl-heptane-3,4-diol (0.1 mmol) was reacted with 3-carbamoyl-5-dipropylcarbamoyl-benzoic acid as described in method A (addition of an extra equivalent of DIEA to neutralize the amine salt) to give N1-[(1S,2R,3R)-1-benzyl-2,3-dihydroxy-6-phenylhexyl]-N3 ,N3-dipropylbenzene-1,3,5-tricarboxamide. MS (ESI+) for C34H43N3O5 m/z 574 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06906104B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-02e36555de4440ef9046f6b7949adf46 |
| Source note | uspto-grants-2005_06 |