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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1071831Generated: November 4, 2026

Diisopropylethylamine → HCID 10120784, compound

https://huagongshe.com/reaction/1071831

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
ReactantTrifluoroacetateHCID 84468—
Reactant3-Carbamoyl-5-dipropylcarbamoyl-benzoic acidHCID 22394891—
ReactantHCID 59067288HCID 59067288—
ProductHCID 10120784HCID 10120784—

Reaction Steps

The trifluoroacetate salt of (2S,3R,4R)-2-amino-1,7-diphenyl-heptane-3,4-diol (0.1 mmol) was reacted with 3-carbamoyl-5-dipropylcarbamoyl-benzoic acid as described in method A (addition of an extra equivalent of DIEA to neutralize the amine salt) to give N1-[(1S,2R,3R)-1-benzyl-2,3-dihydroxy-6-phenylhexyl]-N3 ,N3-dipropylbenzene-1,3,5-tricarboxamide. MS (ESI+) for C34H43N3O5 m/z 574 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06906104B2
Source datasetuspto-grants-2005_06
ORD IDord-02e36555de4440ef9046f6b7949adf46
Source noteuspto-grants-2005_06