HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22390438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 9866911 | HCID 9866911 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22390438 | HCID 22390438 | 59% |
Reaction Steps
3.6 g of the compound of EXAMPLE 1 are hydrogenated in the presence of 0.36 g of 10% palladium on charcoal and 50 ml of ethanol. The reaction mixture is filtered, and the filtrate is evaporated off under reduced pressure. The oily residue obtained is taken up in diethyl ether and hydrochloric acid is bubbled through. The precipitate obtained is filtered off and dried; yield=59%; m.p.=215° C. (HCl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06908914B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-e81d8af4821d4b84a2a286f825373bcd |
| Source note | uspto-grants-2005_06 |