HRID1072239

反应详情

EQUATION

反应方程式

HRID 1072239 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 4-methoxy-3-(4-methoxyphenyl)benzenecarboxaldehyde (1 g, 4.13 mmol) in methanol (12 mL) was treated with polymer-supported borohydride (10.3 mmol) and the mixture shaken for 16 hours. The resin was then filtered and the filtrate concentrated under reduced pressure to afford 0.88 g of title compound.

WORKUP

后处理

  1. filtrationThe resin was then filtered
  2. concentrationthe filtrate concentrated under reduced pressure