HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyltin Chloride → 7-(Thiophen-2-yl)carbonyl-2-(tri-n-butylstannyl)imidazo[5,1-b]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyltin Chloride | HCID 15096 | — |
| Reactant | 7-(Thiophen-2-yl)carbonylimidazo[5,1-b]thiazole | HCID 22390309 | — |
| Reactant | LiHMDS tetrahydrofuran | HCID 23714775 | — |
| Product | 7-(Thiophen-2-yl)carbonyl-2-(tri-n-butylstannyl)imidazo[5,1-b]thiazole | HCID 22390174 | — |
Reaction Steps
The title compound (923 mg) was prepared in substantially the same manner as in step c) of Synthesis Example 1, except that 550 mg of 7-(thiophen-2-yl)carbonylimidazo[5,1-b]thiazole, 0.701 ml of tri-n-butylstannyl chloride, and 3.6 ml of a 1.0 N lithium bis(trimethylsilyl)amide/THF solution were used as the starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06908913B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-65dd41c4d9334c588bd981090b28a8b9 |
| Source note | uspto-grants-2005_06 |