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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072347Generated: November 2, 2026

Tributyltin Chloride → HCID 22390372, compound

https://huagongshe.com/reaction/1072347

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin ChlorideHCID 15096—
ReactantHCID 22390245HCID 22390245—
ReactantLiHMDS tetrahydrofuranHCID 23714775—
ProductHCID 22390372HCID 22390372—

Reaction Steps

The title compound (857 mg) was prepared in substantially the same manner as in step c) of Synthesis Example 1, except that 667 mg of 7-[5-(2-azidoethylthio)pyridin-3-yl]carbonylimidazo[5,1-b]-thiazole, 0.603 ml of tri-n-butylstannyl chloride, and 3.7 ml of a 1.0 N lithium bis(trimethylsilyl)amide/THF solution were used as the starting materials.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06908913B2
Source datasetuspto-grants-2005_06
ORD IDord-2949860bb38f4fafa912ff1162a56c14
Source noteuspto-grants-2005_06