HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyltin Chloride → HCID 86591210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyltin Chloride | HCID 15096 | — |
| Reactant | LiHMDS tetrahydrofuran | HCID 23714775 | — |
| Reactant | HCID 86591211 | HCID 86591211 | — |
| Product | HCID 86591210 | HCID 86591210 | — |
Reaction Steps
The title compound (321 mg) was prepared in substantially the same manner as in step c) of Synthesis Example 1, except that 585 mg of 7-[(2S,4S)-4-azido-1-(4-nitrobenzyloxycarbonyl)pyrrolidin-2-yl]carbonylimidazo[5,1-b]thiazole, 0.396 ml of tri-n-butylstannyl chloride, and 2.8 ml of a 1.0 N lithium bis(trimethylsilyl)amide/THF solution were used as the starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06908913B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-25ad5ccf70a54de780449b62d565a3e3 |
| Source note | uspto-grants-2005_06 |