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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072351Generated: November 4, 2026

Tributyltin Chloride → HCID 86591210, compound

https://huagongshe.com/reaction/1072351

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin ChlorideHCID 15096—
ReactantLiHMDS tetrahydrofuranHCID 23714775—
ReactantHCID 86591211HCID 86591211—
ProductHCID 86591210HCID 86591210—

Reaction Steps

The title compound (321 mg) was prepared in substantially the same manner as in step c) of Synthesis Example 1, except that 585 mg of 7-[(2S,4S)-4-azido-1-(4-nitrobenzyloxycarbonyl)pyrrolidin-2-yl]carbonylimidazo[5,1-b]thiazole, 0.396 ml of tri-n-butylstannyl chloride, and 2.8 ml of a 1.0 N lithium bis(trimethylsilyl)amide/THF solution were used as the starting materials.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06908913B2
Source datasetuspto-grants-2005_06
ORD IDord-25ad5ccf70a54de780449b62d565a3e3
Source noteuspto-grants-2005_06