HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 10132502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 9840705 | HCID 9840705 | — |
| Reactant | 3-Aminophenylboronic acid monohydrate | HCID 14389423 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10132502 | HCID 10132502 | 82.2% |
Reaction Steps
The title compound (230 mg, 82%) was prepared from [2-(4-bromophenoxy)propyl][(methylethyl)sulfonyl]amine (270 mg, 0.803 mmol, prepared in example 1), 3-aminobenzeneboronic acid monohydrate (150 mg, 0.968 mmol), tetrakis(triphenylphosphine)palladium(0) (5 mg, 0.004 mmol), 2 M sodium carbonate (290 mg in 1.4 mL water) and 1,4-dioxane (5.5 mL) in a manner analogous to the procedure described in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911476B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-71f2c0890cb04e04a511327f0efc59e9 |
| Source note | uspto-grants-2005_06 |