HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14853717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethoxalyl chloride | HCID 20884 | — |
| Reactant | N~2~-(Propan-2-yl)pyridine-2,3-diamine | HCID 21818971 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14853717 | HCID 14853717 | — |
Reaction Steps
To a stirred solution of 3-amino-2-isopropylamino-pyridine (2.0 g, 10.6 mmole) and triethylamine (4.8 ml, 34.6 mmole) in tetrahydrofuran (30 ml) was dropwise added ethoxalyl chloride (2.68 ml, 24 mmole). Stirring was continued for two hours after the addition. The mixture was filtered through a glass filter funnel and the filtrate was evaporated to give the title compound as white crystals. M.p. 246°-247° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04968682 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-c3efe739163c4d1384777b2d237f57ca |
| Source note | uspto-grants-1990_11 |