5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine → HCID 67860895, compound

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Reaction Steps

A solution of 2·14 g (10 mmol) of 2-[[[5-[(dimethylamino)methyl]-2-furanyl]methyl]thio]ethylamine and 2·57 g (10 mmol) of 1,1-diphenoxy-2-nitroethene in 20 ml of acetonitrile is boiled for 2 hours. After concentration of the solution by evaporation under vacuum, the oily residue is chromatographically purified as described in Example 1 and yields 3·06 g (81%) of the title compound as a pale yellow oil which according to thin layer chromatography and 1H-NMR spectrum is identical to the compound from Example 1.

Provenance & Evidence