Pyridine → HCID 14552672, compound

HRID 1073429Notes

Reaction equation

HRID 1073429 reaction equation
[CH3:1][C:2]([CH3:17])=[CH:3][CH2:4][O:5][C:6]1[CH:16]=[CH:15][C:9]([O:10][CH:11]([CH3:14])[CH2:12][NH2:13])=[CH:8][CH:7]=1.Cl[C:19]([O:21][CH2:22][CH3:23])=[O:20].N1C=CC=CC=1>>[CH3:17][C:2]([CH3:1])=[CH:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([O:10][CH:11]([CH3:14])[CH2:12][NH:13][C:19](=[O:20])[O:21][CH2:22][CH3:23])=[CH:15][CH:16]=1

Participants

4

Reactant 3

HCID 1049PyridineHCID 10928Ethyl chloroformateHCID 15662564HCID 15662564, compound

Product 1

HCID 14552672HCID 14552672, compound

Procedure

Following the procedure of Example 8, the above propylamine (2.0 g, 8.5 mmol) and ethyl chloroformate (1.01 g, 9.35 mmol) are reacted together, in the presence of pyridine (0.74 g, 9.35 mmol), to give ethyl N-{2-[4-(3-methyl-2-butenoxy)phenoxy]propyl}carbamate, MS m/e 307 (M+).

Sources & evidence

ORD record
ord-4de18bcda0854263b5829d74a9de2976
Source dataset
uspto-grants-1990_11
Patent number
US04968829

Reaction notes

Loading…