HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-[2-(4-Phenoxyphenoxy)ethoxy]pyridinium hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-[2-(4-Phenoxyphenoxy)ethoxy]pyridine | HCID 9948505 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-[2-(4-Phenoxyphenoxy)ethoxy]pyridinium hydrochloride | HCID 22157547 | — |
Reaction Steps
Excess of gaseous hydrogen chloride was gradually introduced into a solution of 2-[2-(4-phenoxyphenoxy)ethoxy]pyridine (1.54 mg, 5.0 mmol) in toluene (50 ml) with stirring. The produced white precipitate was collected by filtration, washed with toluene several times and dried to give 2-[2-(4-phenoxyphenoxy)ethoxy]pyridinium hydrochloride (1.65 g) as white crystals. M.P., 138.1° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04970222 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-689c5bfab8354c1d8810598c22febbb6 |
| Source note | uspto-grants-1990_11 |