HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(5-Cholesten-3beta-yloxy)hexyl iodide → Pregn-5-en-20-one-3beta-yl 6-iodohexyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(5-Cholesten-3beta-yloxy)hexyl iodide | HCID 12805525 | — |
| Reactant | 6-(pregn-5-en-20-one-3beta-yloxy)hexyl 1-thio-beta-D-mannopyranoside | HCID 86741363 | — |
| Product | Pregn-5-en-20-one-3beta-yl 6-iodohexyl ether | HCID 86741362 | — |
Reaction Steps
Employing the procedure substantially as described in Example 2, but substituting for cholest-5-en-3β-yl 6-iodohexyl ether, an equivalent amount of pregn-5-en-20-one-3β-yl 6-iodohexyl ether, there was prepared 6-(Pregn-5-en-20-one-3β-yloxy)hexyl 1-thio-β-D-mannopyranoside (Step D). TLC data and Rf values are given in the above Table.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04970199 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-6631f420aef94c579a83c6c25c0c1ac7 |
| Source note | uspto-grants-1990_11 |