HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-Hexyl-2-cyclopenten-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Product | 2-Hexyl-2-cyclopenten-1-one | HCID 66768 | 97% |
Reaction Steps
The above prepared mixture (25 parts) was admixed with p-toluenesulfonic acid (1.25 parts) and toluene (75 parts) and refluxed for 2 hours, during which by-produced water was eliminated by azeotropic distillation. The reaction mixture was treated as in Example 1 to give 2-n-hexyl-2-cyclopentenone in a yield of 97 %.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04970345 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-f0a1d5ac81a641f29422c21b54eac18b |
| Source note | uspto-grants-1990_11 |