m-Chloroperbenzoic acid → HCID 14229238, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 9.8 g of N-methyl-N-(2-phenyl-2-propenyl)-p-toluenesulfonamide, 9.63 g of m-chloroperbenzoic acid and 280 ml of chloroform were stirred at 60° C. for 3 hours. After cooling, the reaction mixture was washed subsequently with 10% aqueous sodium bisulfite and water, dried over anhydrous magnesium sulfate. The solvent was distilled off and the residue was purified by silica gel column chromatography (developing solvent:ethyl acetate -n-hexane) to obtain 7.7 g of the titled compound.

Provenance & Evidence