Acetonitrile → HCID 14075466, compound

HRID 1073768Notes

Reaction equation

Cl[C:2]1[CH:3]=[CH:4][C:5]2[N:11]([C:12](=[O:26])[CH2:13][N:14]3[CH2:19][CH2:18][CH2:17][CH2:16][CH:15]3[CH2:20][N:21]([CH2:24][CH3:25])[CH2:22][CH3:23])[C:10]3[N:27]=[CH:28][CH:29]=[CH:30][C:9]=3[NH:8][C:7](=[O:31])[C:6]=2[CH:32]=1.[C:33](#N)C>>[CH2:24]([N:21]([CH2:20][CH:15]1[CH2:16][CH2:17][CH2:18][CH2:19][N:14]1[CH2:13][C:12]([N:11]1[C:5]2[CH:4]=[CH:3][CH:2]=[CH:32][C:6]=2[C:7](=[O:31])[NH:8][C:9]2[CH:30]=[CH:29][C:28]([CH3:33])=[N:27][C:10]1=2)=[O:26])[CH2:22][CH3:23])[CH3:25]

Participants

Reactant 2

HCID 6342Acetonitrile

HCID 14590401HCID 14590401, compound

Product 1

HCID 14075466HCID 14075466, compound

Procedure

8-Chloro-11-[[2-[(diethylamino)methyl]-1-piperidinyl]acetyl]-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one of m.p. 186° to 188° C. (acetonitrile using active charcoal);

Sources & evidence

ORD record: ord-49002b79fed94258bd979ba0b6c0e3c9
Source dataset: uspto-grants-1990_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04971966

Reaction notes

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