HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 73861457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 22902739 | HCID 22902739 | — |
| Product | HCID 73861457 | HCID 73861457 | — |
Reaction Steps
Following the general procedure of Example 1, the title compound is prepared from 1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-one oxime (2.7 g, 10 mmol) and 1.1 g (10 mmol) of benzaldehyde in a yield of 2.0 g (56%) as a white solid after flash chromatography on silica gel (8:1, heptane:ethyl acetate) which solid melts at 149°-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04972009 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-7fbb5a50b8524b1b8b32b5076418d889 |
| Source note | uspto-grants-1990_11 |