HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → alpha-[(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)aminocarbonyl)-methyl]-N-[2-(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)-aminocarbonyl)ethyl]nitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | N,N-bis[2-(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)aminocarbonyl)ethyl]hydroxylamine | HCID 22902719 | — |
| Reactant | N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)acrylamide | HCID 22902734 | — |
| Product | alpha-[(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)aminocarbonyl)-methyl]-N-[2-(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)-aminocarbonyl)ethyl]nitrone | HCID 86744352 | — |
Reaction Steps
Following the general procedure of Example 6, the title compound is prepared from N,N-bis[2-(N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)aminocarbonyl)ethyl]hydroxylamine. This intermediate is prepared from N,N-bis(2,2,6,6-tetramethylpiperidin-4-yl)acrylamide and hydroxylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04972009 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-53055fb42621422c8dbf8accb1c72ecd |
| Source note | uspto-grants-1990_11 |