Octadecylamine → HCID 22155759, compound

HRID 1074124Notes

Reaction equation

HRID 1074124 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([N+:11]([O-:13])=[O:12])=[CH:4][N:3]=1.[CH2:14]([NH2:32])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]>>[CH2:14]([NH:32][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([N+:11]([O-:13])=[O:12])=[CH:4][N:3]=1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]

Participants

3

Reactant 2

HCID 15793OctadecylamineHCID 757382-Chloro-3,5-dinitropyridine

Product 1

HCID 22155759HCID 22155759, compound

Procedure

The synthesis is carried out analogously to Example 1 using 2-chloro-3,5-dinitropyridine (Fluka) and octadecylamine as the starting materials. Octadecylamine is recrystallized several times from ethanol before the synthesis.

Workup

  1. customOctadecylamine is recrystallized several times from ethanol
  2. custombefore the synthesis

Sources & evidence

ORD record
ord-eef0dac900244def896805b5f8a13f72
Source dataset
uspto-grants-1990_11
Patent number
US04973429

Reaction notes

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