HCID 14459255, compound → HCID 14459256, compound

HRID 1074170Notes

Reaction equation

HRID 1074170 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=O)[CH2:9][N:10]([CH3:20])[C:11]([NH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:12])=[CH:4][CH:3]=1>C(O)(=O)C>[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:13]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:11](=[O:12])[N:10]([CH3:20])[CH:9]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 14459255HCID 14459255, compound

Product 1

HCID 14459256HCID 14459256, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

3.5 g (12.2 mmol) of the compound from Example 3 are heated under reflux for 24 hours in 50 ml of glacial acetic acid, the solvent is removed and the residue is washed with water. After drying 3.12 g are obtained.

Workup

  1. customthe solvent is removed
  2. washthe residue is washed with water
  3. customAfter drying 3.12 g
  4. customare obtained

Sources & evidence

ORD record
ord-63043783a2d24172825c04251031b999
Source dataset
uspto-grants-1990_11
Patent number
US04973598

Reaction notes

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